• 专利标题:   Preparation of graphene oxide/iron oxide/silver nanocomposite absorbing material involves mixing graphene oxide aqueous and sodium hydroxide aqueous solution, heating at specific conditions, and adjusting pH to specific range.
  • 专利号:   CN103305185-A, CN103305185-B
  • 发明人:   HUANG Y, ZHANG N, ZONG M, LUO D, WANG S, QU C, ZHENG J
  • 专利权人:   UNIV NORTHWESTERN POLYTECHNICAL
  • 国际专利分类:   C09K003/00
  • 专利详细信息:   CN103305185-A 18 Sep 2013 C09K-003/00 201381 Pages: 9 Chinese
  • 申请详细信息:   CN103305185-A CN10229123 08 Jun 2013
  • 优先权号:   CN10229123

▎ 摘  要

NOVELTY - Preparation of graphene oxide/iron oxide/silver nanocomposite absorbing material involves mixing 0.2-2 mg/ml graphene oxide aqueous and 0.5-5 mol/L sodium hydroxide aqueous solution, heating at 30-50 degrees C for 10 minutes under water bath condition, adjusting pH to 9-12, further heating to 60-80 degrees C for 2-3 hours, centrifuging and obtaining black precipitate, washing precipitate 3-5 times using deionized water, adding silver nitrate, stirring for 20 minutes, adding sodium borohydride dissolved in 50-200 ml water, and heating at 20-100 degrees C for 0.5-2 hours. USE - Preparation of graphene oxide/iron oxide/silver nanocomposite absorbing material (claimed). ADVANTAGE - The method efficiently and economically provides graphene oxide/iron oxide/silver nanocomposite absorbing material effectively adsorbs different wavelengths. DETAILED DESCRIPTION - Preparation of graphene oxide/iron oxide/silver nanocomposite absorbing material involves mixing 0.2-2 mg/ml graphene oxide aqueous and 0.5-5 mol/L sodium hydroxide aqueous solution in mass ratio of 1:x:(0.8-1.8)x, where x is 0.1-10, heating at 30-50 degrees C for 10 minutes under water bath condition, adjusting pH to 9-12, further heating to 60-80 degrees C for 2-3 hours, centrifuging and obtaining black precipitate, washing precipitate 3-5 times using deionized water, adding silver nitrate, stirring for 20 minutes, adding sodium borohydride dissolved in 50-200 ml water, heating at 20-100 degrees C for 0.5-2 hours, washing obtained product using deionized water and ethanol, magnetically-separating, centrifuging or filtering and obtaining black precipitate, and vacuum-drying precipitate at 40-80 degrees C.