• 专利标题:   Preparation of high-dispersibility graphene-loaded tin-dioxide nanoparticles-containing composite material involves mixing graphite oxide with ethylene glycol, adding water and liquid stannous chloride, and heating liquid mixture.
  • 专利号:   CN104528701-A, CN104528701-B
  • 发明人:   GAO Y, YIN G, QU Y
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   B82Y030/00, C01B031/04, C01G019/02
  • 专利详细信息:   CN104528701-A 22 Apr 2015 C01B-031/04 201546 Pages: 7 Chinese
  • 申请详细信息:   CN104528701-A CN10809858 23 Dec 2014
  • 优先权号:   CN10809858

▎ 摘  要

NOVELTY - Graphite oxide is mixed with ethylene glycol, and ultrasonically-mixed for 1-2 hours, to obtain graphene oxide solution. The volume ratio of graphite oxide and ethylene glycol is 1-4 mg:1-4 mL. Predetermined amount of water is added to graphene oxide solution to form dilute graphite oxide solution, and ultrasonically-mixed for 10-30 minutes. Predetermined amount of liquid stannous chloride is added and ultrasonically-mixed for 10-30 minutes. The liquid mixture is heated in oil bath, to obtain high-dispersibility graphene-loaded tin-dioxide nanoparticles-containing composite material. USE - Preparation of high-dispersibility graphene-loaded tin-dioxide nanoparticles-containing composite material (claimed). ADVANTAGE - The method enables preparation of high-dispersibility graphene-loaded tin-dioxide nanoparticles-containing composite material by simple method, without agglomeration. DETAILED DESCRIPTION - Graphite oxide is mixed with ethylene glycol, and ultrasonically-mixed for 1-2 hours, to obtain graphene oxide solution. The volume ratio of graphite oxide and ethylene glycol is 1-4 mg:1-4 mL. Predetermined amount of water is added to graphene oxide solution to form dilute graphite oxide solution, and ultrasonically-mixed for 10-30 minutes. Predetermined amount of liquid stannous chloride is added and ultrasonically-mixed for 10-30 minutes. The volume ratio of stannous chloride and water is 10-50 mg: 1 mL. The mass ratio of stannous chloride and graphite oxide is 1:2-4. The liquid mixture is heated in oil bath, to obtain high-dispersibility graphene-loaded tin-dioxide nanoparticles-containing composite material.