• 专利标题:   Reinforced graphene composite aerogel useful for thermal protection requirements of aircraft in high-temperature environment, comprises two-dimensional nanographene sheet, and two-dimensional nano-graphene sheet loaded with nano-scale silicon carbon-nitride-aluminum oxide ceramic particles.
  • 专利号:   CN114956834-A
  • 发明人:   CHEN J, CHU X, SUI Y, LIU W, YUAN W, LIU H
  • 专利权人:   UNIV TIANJIN CHENGJIAN
  • 国际专利分类:   B01J013/00, C04B035/117, C04B035/589, C04B035/596, C04B035/622, C04B038/00
  • 专利详细信息:   CN114956834-A 30 Aug 2022 C04B-035/589 202290 Chinese
  • 申请详细信息:   CN114956834-A CN10665903 14 Jun 2022
  • 优先权号:   CN10665903

▎ 摘  要

NOVELTY - Reinforced graphene composite aerogel comprises two-dimensional nanographene sheets, where the two-dimensional nano-graphene sheet is loaded with nano-scale silicon carbon-nitride-aluminum oxide ceramic particles, the silicon carbon-nitride-aluminum oxide ceramic particles is connected to each other, and form a nano-interpenetrating structure with two-dimensional nano-graphene sheet, the silicon carbon-nitride-aluminum oxide ceramic particles and two-dimensional nano-graphene sheet form a porous skeleton network, and the porous framework network has nano-scale uniform pores. USE - The reinforced graphene composite aerogel is useful for thermal protection requirements of aircraft in high-temperature environment. ADVANTAGE - The aerogel has porous skeleton network, nano-scale uniform pores, excellent mechanical properties and good high-temperature thermal insulation properties, which can meet thermal protection requirements of aircraft in high-temperature environments. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparing reinforced graphene composite aerogel, comprising choosing graphene oxide and polysilazane ceramic precursors as raw materials, using aluminum-tri-sec-butoxide as an aluminum source, and divinylbenzene as a cross-linking agent, adding an organic solvent to obtain wet gel by hydrothermal reaction, drying wet gel by supercritical carbon dioxide to obtain ceramic precursor/reduced graphene oxide aerogel, high temperature cracking, and converting ceramic precursor aerogel into ceramic aerogel to obtain silicon carbon-nitride-aluminum oxide/rGO composite aerogel.