• 专利标题:   Preparation of high performance graphene porous film used for e.g. solar energy battery, by taking graphene oxide and water, mixing, ultrasonically dispersing, extruding, coagulating, in situ growing inorganic crystals, and reducing.
  • 专利号:   CN104609410-A
  • 发明人:   GAO C, LIU Z, HUANG T
  • 专利权人:   ZHEJIANG TANGU SHANGXI MATERIAL TECHNOLO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104609410-A 13 May 2015 C01B-031/04 201555 Pages: 13 Chinese
  • 申请详细信息:   CN104609410-A CN10049657 30 Jan 2015
  • 优先权号:   CN10049657

▎ 摘  要

NOVELTY - A high performance graphene porous film is prepared by taking 1 pt. wt. graphene oxide and 5-150 pts. wt. water, mixing, ultrasonically dispersing to obtain graphene oxide dispersion liquid, extruding into A-shaped die extrusion device at speed of 10-1000 mL/hour, coagulating with coagulating liquid at 10-80 degrees C for 1-100 seconds to graphene oxide hydrogel film, in situ growing inorganic crystals into precipitating agent for 0.1-8 hours to obtain graphene oxide film, reducing with reducing agent at 80-95 degrees C for 1-8 hours, and stucking into dissolving agent for 1-8 hours. USE - Method for preparing high performance graphene porous film (claimed) used for solar energy battery, supercapacitor and lithium ion battery energy storage field. ADVANTAGE - The method is simple, green and environment-friendly, and has low energy consumption. The product has high conductivity, good surface area and pore volume.