• 专利标题:   Preparation of graphene involves grinding pure magnesium powder, mixing magnesium powder with sodium chloride, adding carbon tetrachloride liquid to another ceramic container, and vacuumizing mixture in vacuum furnace.
  • 专利号:   CN106517156-A
  • 发明人:   CHEN Z, ZHU H, ZHANG Z
  • 专利权人:   UNIV CHANGSHA SCI TECHNOLOGY
  • 国际专利分类:   C01B025/45, C01B032/184
  • 专利详细信息:   CN106517156-A 22 Mar 2017 C01B-032/184 201731 Pages: 5 Chinese
  • 申请详细信息:   CN106517156-A CN10954267 03 Nov 2016
  • 优先权号:   CN10954267

▎ 摘  要

NOVELTY - The preparation method of graphene involves grinding more than 90% pure magnesium powder into 200 mesh particles, mixing magnesium powder with sodium chloride, placing the mixture in ceramic container, adding carbon tetrachloride liquid to another ceramic container, vacuumizing the mixture in vacuum furnace at atmospheric pressure of 10 Pa and temperature of 500-550 degrees C, carrying out reduction reaction of carbon tetrachloride with magnesium powder for 1-3 hours, dissolving reaction product in hydrochloric acid and filtering. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method enables simple and economical preparation of graphene with high purity.