• 专利标题:   Preparation method of bonding mortar for high temperature and high humidity condition, involves adding prepared polyvinyl alcohol functionalized oxide/graphene oxide composite material, quartz sand and defoamer.
  • 专利号:   CN115947574-A
  • 发明人:   FAN S, HU Y, AN Y
  • 专利权人:   LINHAI ZHONGXIN NEW BUILDING MATERIALS
  • 国际专利分类:   C04B014/06, C04B014/36, C04B014/46, C04B018/02, C04B020/02, C04B028/04
  • 专利详细信息:   CN115947574-A 11 Apr 2023 C04B-028/04 202340 Chinese
  • 申请详细信息:   CN115947574-A CN11719248 30 Dec 2022
  • 优先权号:   CN11719248

▎ 摘  要

NOVELTY - Method for preparing adhesive mortar suitable for high-temperature and high-humidity conditions involves (a) mixing graphene oxide and deionized water and ultrasonicating, adding cetyltrimethylammonium bromide and ethyl orthosilicate to the graphene oxide dispersion to carry out hydrolysis reaction, cooling to room temperature after the reaction finishes, filtering the reaction solution, and washing the filtered precipitate with deionized water and drying, (b) mixing the above-mentioned graphene oxide/silicon oxide composite material and polyvinyl alcohol solution, ultrasonically treating at room temperature, filtering and drying, and (c) adding basalt fiber, fly ash, and cement into the mixer for the first mixing, adding the above-mentioned polyvinyl alcohol functionalized graphene oxide/silicon oxide composite material, quartz sand and defoamer, redispersible latex powder, hydroxypropyl methylcellulose ether. USE - Method is used for preparing adhesive mortar suitable for high-temperature and high-humidity conditions (claimed) including insulating plate, ceramic tile, cement-based material agglomerant. ADVANTAGE - The method provides bonding mortar with high bonding strength, durability and functionality, volcanic ash activity of silicon oxide, and improved performance in high temperature and high humidity environment. The modified polyvinyl alcohol improves the performance of the bonding mortar to a certain extent. DETAILED DESCRIPTION - Method for preparing adhesive mortar suitable for high-temperature and high-humidity conditions involves (a) mixing graphene oxide and deionized water and ultrasonicating to obtain a graphene oxide dispersion, adding cetyltrimethylammonium bromide and ethyl orthosilicate to the graphene oxide dispersion to carry out hydrolysis reaction, cooling to room temperature after the reaction finishes, filtering the reaction solution, and washing the filtered precipitate with deionized water and drying to obtain a graphene oxide/silicon oxide composite material, (b) mixing the above-mentioned graphene oxide/silicon oxide composite material and polyvinyl alcohol solution, ultrasonically treating at room temperature, filtering and drying to obtain a polyvinyl alcohol functionalized graphene oxide/silicon oxide composite material, and (c) adding basalt fiber, fly ash, and cement into the mixer for the first mixing, adding the above-mentioned polyvinyl alcohol functionalized graphene oxide/silicon oxide composite material, quartz sand and defoamer, redispersible latex powder, hydroxypropyl methylcellulose ether, and carrying out the second stirring and mixing to prepare the bonding mortar. An INDEPENDENT CLAIM is included for the adhesive mortar suitable for high-temperature and high-humidity conditions obtained by the above-mentioned method.