• 专利标题:   Preparing graphene modified expanded filament, comprises performing esterification reaction on phthalic acid and ethylene glycol, and dissolving graphene copolymerization modified polyethylene terephthalate in phenol and tetrachloroethane solution.
  • 专利号:   CN114214754-A
  • 发明人:   JIANG H, ZHOU L, JIANG S
  • 专利权人:   CHANGZHOU LINGDA SPECIAL FIBER CO LTD
  • 国际专利分类:   D01F001/09, D01F001/10, D01F006/92
  • 专利详细信息:   CN114214754-A 22 Mar 2022 D01F-006/92 202253 Chinese
  • 申请详细信息:   CN114214754-A CN11585656 23 Dec 2021
  • 优先权号:   CN11585656

▎ 摘  要

NOVELTY - Preparing graphene modified expanded filament, comprises (1) performing esterification reaction on phthalic acid and ethylene glycol, adding diladder trioxide, triphenyl phosphite and deionized water, and stirring into slurry; (2) adding ethylene glycol terephthalate and graphene oxide into polymerization kettle, when adding, opening nitrogen, stirring graphene copolymerization modified polyethylene terephthalate and graphene oxide, stirring uniformly, heating and opening vacuum pump to obtain graphene modified polyethylene terephthalate; (3) dissolving graphene copolymerization modified polyethylene terephthalate in phenol and tetrachloroethane solution, adding into centrifuge, taking out precipitate, heating and dissolving for 2 hours in tetrachloroethane solution, and centrifuging to obtain final precipitate; and (4) repeatedly washing precipitate by methanol, filtering, spinning, solidifying, stretching, water washing, bleaching, oiling, drying, and rolling. USE - The method is useful for preparing graphene modified expanded filament. ADVANTAGE - The expanded filament has multifunctional integrated filaments e.g. antibacterial, anti-ultraviolet, antistatic and moisture absorption, and has wider range of use.