• 专利标题:   Preparation of graphene oxide nanofiltration membrane, involves adding concentrated sulfuric acid, potassium permanganate, hydrogen peroxide solution, and preparing graphene oxide aqueous solution by modified Hummmers method.
  • 专利号:   CN110075710-A
  • 发明人:   SHA Y, SHA X
  • 专利权人:   NANTONG QIANGSHENG GRAPHENE TECHNOLOGY
  • 国际专利分类:   B01D061/02, B01D067/00, B01D069/12, B01D071/02, B01D071/16, B01D071/26, B01D071/30, B01D071/34, B01D071/42, B01D071/48, B01D071/56, B01D071/68
  • 专利详细信息:   CN110075710-A 02 Aug 2019 B01D-061/02 201977 Pages: 10 Chinese
  • 申请详细信息:   CN110075710-A CN10223959 22 Mar 2019
  • 优先权号:   CN10223959

▎ 摘  要

NOVELTY - The preparation of graphene oxide nanofiltration membrane involves (S1) using expanded graphite as raw material, adding concentrated sulfuric acid, potassium permanganate, hydrogen peroxide solution, and preparing a graphene oxide aqueous solution by modified Hummmers method, (S2) adding an amine monomer to the aqueous graphene oxide solution to prepare an aqueous graphene oxide casting solution, (S3) using a high molecular polymer ultrafiltration membrane as a base film, dip coating a layer of graphene oxide aqueous casting solution on the base film by surface coating method, the dip coating time is 1-5 minutes, re-dip coating a layer of oil, the dip coating time is 1-30 minutes, performing interfacial polymerization of the graphene oxide aqueous casting solution and the oil phase monomer, and drying at 60-100 degrees C for 5-10 hours. USE - Preparation of graphene oxide nanofiltration membrane. ADVANTAGE - The cleaning effect is achieved after parallel washing, so that the nanofiltration membrane has excellent filtering ability and stain resistance, thus significantly improving the service life.