• 专利标题:   Preparation of graphene/lithium titanium phosphate lithium battery cathode material by preparing precursor including lithium carbonate, monoammonium phosphate, and titanium dioxide, heating, plating, dipping in dilute acid, and drying.
  • 专利号:   CN108666551-A
  • 发明人:   CHEN Q, ZHAO H
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   H01M004/36, H01M004/58, H01M004/62, H01M010/36
  • 专利详细信息:   CN108666551-A 16 Oct 2018 H01M-004/36 201901 Pages: 10 Chinese
  • 申请详细信息:   CN108666551-A CN10397079 28 Apr 2018
  • 优先权号:   CN10397079

▎ 摘  要

NOVELTY - Preparation of a graphene/lithium titanium phosphate (LiTi2(PO4)3) lithium battery cathode material comprises dissolving polyvinyl alcohol in deionized water, placing in a 80 degrees C water bath, adding lithium carbonate, monoammonium phosphate, and titanium dioxide, stirring to completely dissolve, pre-calcining to form solid, drying and grinding it to obtain a precursor, placing the precursor in a tubular furnace, under the protection of argon atmosphere, heating to 900-950 degrees C, preferably 930 degrees C at 8-12 degrees C/minute, preferably 10 degrees C/minute, and keeping the temperature for 8-12 hours to obtain a composite; plating the composite surface with a hydrogenated metal film having a thickness of 0.2-0.8 mu m; pre-heating to 500-800 degrees C, introducing carbon source gas, heating to 900-1200 degrees C, cooling to room temperature, taking out, removing metal by dipping in dilute acid, washing, and drying at 80 degrees C for 24 hours. USE - Method for preparing a graphene/lithium titanium phosphate (LiTi2(PO4)3) lithium battery cathode material. ADVANTAGE - The lithium battery cathode material has improved conductivity, high-current charging performance, specific capacity of 85%, and prevent generation of the side reaction of electrode material and water, and has improved electrochemical performance and stability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for graphene/LiTi2(PO4)3 lithium battery cathode material.