• 专利标题:   Preparation of graphene/silver/mesoporous titanium dioxide nanocomposite photocatalyst useful for degradation of organic contaminants in sewage or air, involves dissolving graphene oxide and silver nitrate in tetrabutyl titanate.
  • 专利号:   CN105771980-A
  • 发明人:   LI M, LI Y, CHEN F
  • 专利权人:   UNIV JISHOU
  • 国际专利分类:   B01D053/72, B01D053/86, B01J023/50, B01J035/10, C02F001/30, C02F001/32, C02F001/72
  • 专利详细信息:   CN105771980-A 20 Jul 2016 B01J-023/50 201669 Pages: 9 Chinese
  • 申请详细信息:   CN105771980-A CN10267756 27 Apr 2016
  • 优先权号:   CN10267756

▎ 摘  要

NOVELTY - Preparation of graphene/silver/mesoporous titanium dioxide nanocomposite photocatalyst involves dissolving graphene oxide and graphene in an organic solvent and then mixing to obtain a graphene solution, adding silver nitrate solution to the graphene solution and mixing to obtain a graphene/silver solution, dissolving hexadecyltrimethylammonium bromide in an organic solvent and mixing, dissolving tetrabutyl titanate in an organic solvent and mixing, adding nitric acid solution to the mixture and stirring, adding graphene/silver solution to the mixture, and sintering. USE - The process is useful for preparation of graphene/silver/mesoporous titanium dioxide nanocomposite photocatalyst, which is useful for photocatalytic degradation of organic contaminants in sewage or air (claimed). DETAILED DESCRIPTION - Preparation of graphene/silver/mesoporous titanium dioxide nanocomposite photocatalyst involves dissolving graphene oxide and graphene in an organic solvent, uniformly mixing to obtain a graphene solution, adding silver nitrate solution to the graphene solution and then mixing to obtain a graphene/silver solution, dissolving hexadecyltrimethylammonium bromide in an organic solvent, uniformly mixing to obtain a solution (A), dissolving tetrabutyl titanate in an organic solvent to obtain a transparent solution (B), adding solution (B) to the solution (A), uniformly mixing, controlling speed for 0.5-5 seconds to obtain a solution (C), adding nitric acid solution to the solution (C) and then stirring to obtain an inorganic titanium precursor solution (E), adding graphene/silver solution to the solution (E) and then continuously stirring, extracting the mixture and then drying, and sintering under nitrogen atmosphere. INDEPENDENT CLAIMS are included for the following: (1) graphene/silver/mesoporous titanium dioxide nanocomposite photocatalyst prepared by the method; and (2) use of graphene/silver/mesoporous titanium dioxide nanocomposite photocatalyst for photocatalytic degradation of organic contaminants in sewage or air.