• 专利标题:   Modifying composite material involves preparing mixed solvent containing aqueous solution of sodium thiocyanate and sodium nitrate, mixing graphene powder with solvent, and ultra-sonicating obtained mixture to obtain graphene suspension.
  • 专利号:   CN105421036-A, CN105421036-B
  • 发明人:   LUO R, YANG W
  • 专利权人:   UNIV BEIHANG
  • 国际专利分类:   D06B021/00, D06C007/00, D06C007/04, D06M011/74, D06M015/31
  • 专利详细信息:   CN105421036-A 23 Mar 2016 D06M-011/74 201650 Pages: 10 English
  • 申请详细信息:   CN105421036-A CN10982891 23 Dec 2015
  • 优先权号:   CN10982891

▎ 摘  要

NOVELTY - Modifying composite material involves preparing mixed solvent containing aqueous solution of sodium thiocyanate and sodium nitrate in ratio of 1:2-1:5. Graphene powder is mixed with 5-10 wt.% solvent, and then ultra-sonicated for 1-3 hours to obtain graphene suspension. Polyacrylonitrile powder is mixed with solvent for 12-36 hours, and then heated at 50-80 degrees C with stirring to obtain polyacrylonitrile solution. The polyacrylonitrile and solvent are mixed in ratio of 1:3-1:10. The polyacrylonitrile solution is mixed with graphene suspension and mixed solvent with stirring at 50-80 degrees C. USE - Method for modifying composite material (claimed). ADVANTAGE - The method enables to modify composite material that has improved performance at high temperature. DETAILED DESCRIPTION - Modifying composite material involves preparing mixed solvent containing aqueous solution of sodium thiocyanate and sodium nitrate in ratio of 1:2-1:5. Graphene powder is mixed with 5-10 wt.% solvent, and then ultra-sonicated for 1-3 hours to obtain graphene suspension. Polyacrylonitrile powder is mixed with solvent for 12-36 hours, and then heated at 50-80 degrees C with stirring to obtain polyacrylonitrile solution. The polyacrylonitrile and solvent are mixed in ratio of 1:3-1:10. The polyacrylonitrile solution is mixed with graphene suspension and mixed solvent with stirring at 50-80 degrees C for 12-24 hours under vacuum to obtain polyacrylonitrile-modified solution. The obtained polyacrylonitrile-modified solution is placed in vacuum impregnation apparatus at -0.1 mega-pascal vacuum at 80-120 degrees C to obtain modified composite material.