• 专利标题:   Preparing graphene and polyolefin composite material comprises dispersing the graphene oxide in solvent, to obtain suspension liquid, reacting suspension, to obtain foamed graphene precursor, dissolving foamed graphene precursor in water.
  • 专利号:   CN107236148-A, CN107236148-B
  • 发明人:   HOU Y, ZHU B, JIANG R, LU X
  • 专利权人:   PETROCHINA CO LTD
  • 国际专利分类:   C08K003/04, C08K007/24, C08L021/00, C08L023/06, C08L023/12, C08L025/06, C08L033/12, C08L063/00, C08L077/00, C08L079/08, C08L083/04, C08L091/06, C23C016/26, C23C016/44
  • 专利详细信息:   CN107236148-A 10 Oct 2017 C08K-003/04 201782 Pages: 9 Chinese
  • 申请详细信息:   CN107236148-A CN10302879 03 May 2017
  • 优先权号:   CN10302879

▎ 摘  要

NOVELTY - Preparing graphene and polyolefin composite material comprises dispersing the graphene oxide in solvent, to obtain suspension liquid, where the concentration of the suspension liquid is 0.1-10 mg/ml, reacting the suspension at 100-200 degrees C for 12-24 hours, to obtain a foamed graphene precursor, dissolving the foamed graphene precursor in water, freeze-drying at -80 to -10 degrees C, under inert atmosphere at 700-1200 degrees C, roasting for 1-3 hours, to obtain foamed graphene, soaking foamed graphene in a polyolefin solution, evaporating to dryness, to obtain composite material of graphene and polyolefin. USE - The method is useful for preparing graphene and polyolefin composite material (claimed). ADVANTAGE - The material is cheap. The method is produced in large scale. DETAILED DESCRIPTION - Preparing graphene and polyolefin composite material comprises dispersing the graphene oxide in the solvent, to obtain the suspension liquid, where the concentration of the suspension liquid is 0.1-10 mg/ml, reacting the suspension at 100-200 degrees C for 12-24 hours, to obtain a foamed graphene precursor, dissolving the foamed graphene precursor in water, freeze-drying at -80 to -10 degrees C, under an inert atmosphere at 700-1200 degrees C, roasting for 1-3 hours, to obtain a foamed graphene, soaking the foamed graphene in a polyolefin solution, evaporating to dryness, to obtain a composite material of graphene and polyolefin, where the proportion of the foamed graphene in the composite material of the graphene and the polyolefin is 0.01-20 wt.%, and the proportion of polyolefin in the composite material of graphene and polyolefin is 80-99.99 wt.%.