• 专利标题:   Preparation of graphene film under pressure by applying pressure on graphene oxide, placing to high-frequency induction graphitization furnace, vacuumizing, passing through nitrogen protective gas while graphitizing, and removing pressure.
  • 专利号:   CN110540193-A
  • 发明人:   LIU J, ZHANG M, LU X
  • 专利权人:   UNIV SHANGHAI
  • 国际专利分类:   C01B032/184, C01B032/194
  • 专利详细信息:   CN110540193-A 06 Dec 2019 C01B-032/184 202004 Pages: 9 Chinese
  • 申请详细信息:   CN110540193-A CN10890661 20 Sep 2019
  • 优先权号:   CN10890661

▎ 摘  要

NOVELTY - Preparation of graphene film under pressure comprises applying pressure on graphene oxide at not greater than 12 MPa, placing to high-frequency induction graphitization furnace, vacuumizing, passing through nitrogen protective gas while performing graphitization reaction at 2800-3000 degrees C to form non-oxidizing gas atmosphere, and removing oxidative functional groups and metal impurities to obtain graphene film; and removing pressure of graphene film, taking out, and mechanically rolling into desired thickness. USE - The method is for preparation of graphene film under pressure. ADVANTAGE - The method is simple, appplies pressure to graphene film to reduce structural defects caused by the removal of oxygen-containing functional groups inside the film, improves the surface roughness of graphene, increases grain size, and improves mechanical properties, tensile strength, flexibility and surface quality.