• 专利标题:   Preparing functionalized graphene with gas-sensitive performance by preparing sulfonated graphene oxide, hydrothermally reacting with potassium stannate, L-cysteine and cetyltrimethylammonium bromide and forming material with tin sulfide.
  • 专利号:   CN111115619-A, AU2020102360-A4
  • 发明人:   JIAO W, HUANG Y, WANG R, HE X
  • 专利权人:   SHENZHEN XICHUANG ADVANCED MATERIAL INST, HARBIN INST TECHNOLOGY SHENZHEN GRADUATE, SHENZHEN STRONG ADVANCED MATERIALS RES
  • 国际专利分类:   C01B032/184, C01B032/194, C01G019/00, G01N027/12, C09D011/50, G01N033/52
  • 专利详细信息:   CN111115619-A 08 May 2020 C01B-032/184 202046 Pages: 7 Chinese
  • 申请详细信息:   CN111115619-A CN11391696 30 Dec 2019
  • 优先权号:   CN11391696

▎ 摘  要

NOVELTY - Method for preparing functionalized graphene, involves (i) preparing sulfonated graphene oxide and (ii) using potassium stannate as a tin source, L-cysteine as a sulfur source and cetyltrimethylammonium bromide (CTAB) as a dispersant under hydrothermal conditions, where the tin sulfide crystal is crystallized on the surface of the functionalized graphene and forming the functionalized graphene gas-sensitive material loaded with tin sulfide. USE - The method is useful for preparing functionalized graphene with gas-sensitive performance used in a gas-sensitive ink. ADVANTAGE - The method provides the product with excellent dispersion performance in a solvent. The gas-sensitive ink can quickly adsorb nitrogen dioxide and ammonia molecules, has extremely high sensitivity, is not influenced by the external humidity environment, can be directly written on the common substrates such as glass, paper and cloth without the participation of interdigitated electrodes and adopts rapid, simple, repeatable and easily controllable preparation method. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) the functionalized graphene prepared by the method; and (2) a gas-sensitive ink is prepared by adding the functionalized graphene to an ethanol solution and obtaining the product after dispersion.