• 专利标题:   Preparation of graphene involves adding anthracite coal into graphitization furnace, adding acid, oxidizing agent and surface modifier, heating, hydrolyzing, adding hydrogen peroxide, reacting, obtaining graphite oxide and reducing.
  • 专利号:   CN105502364-A, CN105502364-B
  • 发明人:   MA J, XU Y, YANG G, YANG Z, ZHANG J
  • 专利权人:   SHENHUA GROUP CORP LTD, SHENHUA NINGXIA COAL IND GROUP CO LTD, SHENHUA GROUP CORP LTD, SHENHUA NINGXIA COAL IND GROUP CO LTD
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN105502364-A 20 Apr 2016 C01B-031/04 201655 Pages: 7 English
  • 申请详细信息:   CN105502364-A CN11001166 28 Dec 2015
  • 优先权号:   CN11001166

▎ 摘  要

NOVELTY - Preparation of graphene involves adding anthracite coal into a graphitization furnace, obtaining coal-based graphite, adding acid, mixing in an ice-water bath, adding oxidizing agent and surface modifier, stirring, heating the resultant mixture to 45-95 degrees C for 0.5-2 hours, adding deionized water, hydrolyzing, adding hydrogen peroxide, reacting, filtering the resultant reaction mixture, washing the obtained filter cake, controlling content of acid radical ions in the filter cake to 100 ppm or more, drying filter cake, obtaining graphite oxide and reducing the graphite oxide. USE - Preparation of graphene (claimed). ADVANTAGE - The method provides graphene with high yield, by an economical process.