• 专利标题:   Preparation of graphene-based enhanced flame retardant recycled polyester staple fiber involves mixing graphene masterbatch, phosphorus-based flame retardant masterbatch, and recycled polyester material, melting, filtering and melt-spinning.
  • 专利号:   CN104630928-A, CN104630928-B
  • 发明人:   LI L, LIU P, XU D, WANG Z, YAO Z, ZHOU J, YAO R, DU M, YAO T, LAN T
  • 专利权人:   UNIV NANJING AERONAUTICS ASTRONAUTICS
  • 国际专利分类:   D01F001/10, D01F006/92
  • 专利详细信息:   CN104630928-A 20 May 2015 D01F-006/92 201556 Pages: 7 Chinese
  • 申请详细信息:   CN104630928-A CN10079074 13 Feb 2015
  • 优先权号:   CN10079074

▎ 摘  要

NOVELTY - A graphene-based enhanced flame retardant recycled polyester staple fiber is prepared by mixing graphene and surfactant, dispersing, adding polyester powder, granulating, mixing phosphorus-based halogen-free flame retardant and polyester powder, reacting, granulating, mixing graphene masterbatch, phosphorus-based flame retardant masterbatch, and recycled polyester material, vacuum drying, melting in screw extruder, pumping into homogenizing mixer, purifying, pumping into post-secondary filters, filtering, melt-spinning, tow cutting, and packaging. USE - Method for preparing graphene-based enhanced flame retardant recycled polyester staple fiber (claimed). ADVANTAGE - The fiber has good synergistic effect, and fiber quality. The method reduces cost, and increases fiber mechanical property. DETAILED DESCRIPTION - A graphene-based enhanced flame retardant recycled polyester staple fiber is prepared by mixing graphene and surfactant at mass ratio of 1-5:1, dispersing to obtain graphene particles, adding polyester powder, granulating using twin screw extruder to obtain graphene masterbatch, mixing phosphorus-based halogen-free flame retardant and polyester powder, reacting, granulating using twin screw extruder to obtain phosphorus-based flame retardant masterbatch, mixing graphene masterbatch, phosphorus-based flame retardant masterbatch, and recycled polyester material, vacuum drying at 90-140 degrees C, melting in screw extruder, pumping into homogenizing mixer for 30-90 minutes, purifying, pumping into post-secondary filters, filtering, melt-spinning at 275-278 degrees C, tow cutting, and packaging.