• 专利标题:   Preparing adsorbent for absorbing organic pollutants, involves mixing n-butyl titanate with graphene oxide dispersion liquid, heating obtained mixture, increasing temperature, and mixing with aqueous solution of polyethyleneimine.
  • 专利号:   CN105107476-A, CN105107476-B
  • 发明人:   HUANG Z, TIAN L, ZHANG W, CHEN P, JIANG H, LI M
  • 专利权人:   UNIV NANCHANG HANGKONG
  • 国际专利分类:   B01J020/26, B01J020/30, B01J020/34
  • 专利详细信息:   CN105107476-A 02 Dec 2015 B01J-020/26 201609 Pages: 5 English
  • 申请详细信息:   CN105107476-A CN10528117 26 Aug 2015
  • 优先权号:   CN10528117

▎ 摘  要

NOVELTY - Preparing adsorbent involves mixing n-butyl titanate with graphene oxide dispersion liquid gradually. The obtained mixture is heated at 50-55 degrees C, and graphene oxide dispersion liquid is added gradually in 3-4hours. The graphene oxide dispersion liquid is mixed with n-butyl titanate in ratio of 1:75. The temperature of the obtained mixture is increased to 80-85 degrees C at 9.8-10.2 pH. The obtained mixture is added with 20-40mg/mL aqueous solution of polyethyleneimine gradually. The polyethyleneimine and obtained mixture are mixed in ratio of 3:1. The obtained reaction mixture is kept for 1 day. USE - Method for preparing adsorbent (claimed) for absorbing organic pollutants. ADVANTAGE - The method enables to prepare adsorbent that has good adsorption performance, large adsorption area and good application prospects, and is automatic. DETAILED DESCRIPTION - Preparing adsorbent involves mixing n-butyl titanate with graphene oxide dispersion liquid gradually. The obtained mixture is heated at 50-55 degrees C, and graphene oxide dispersion liquid is added gradually in 3-4hours. The graphene oxide dispersion liquid is mixed with n-butyl titanate in ratio of 1:75. The temperature of the obtained mixture is increased to 80-85 degrees C at 9.8-10.2 pH. The obtained mixture is added with 20-40mg/mL aqueous solution of polyethyleneimine gradually. The polyethyleneimine and obtained mixture are mixed in ratio of 3:1. The obtained reaction mixture is kept for 1 day at room temperature. The obtained precipitate is washed to get neutral pH, and then freeze-dried to obtain product i.e. adsorbent.