• 专利标题:   Preparing titanium dioxide/graphene composite nanomaterial, comprises preparing graphite oxide and graphene oxide using normal chemical method, and taking the graphite oxide dispersed into de-ionized water.
  • 专利号:   CN102500352-A, CN102500352-B
  • 发明人:   HUANG B, QIN X, WANG Z, ZHANG X
  • 专利权人:   UNIV SHANDONG
  • 国际专利分类:   B01J021/18, B01J035/10
  • 专利详细信息:   CN102500352-A 20 Jun 2012 B01J-021/18 201256 Pages: 7 Chinese
  • 申请详细信息:   CN102500352-A CN10359664 15 Nov 2011
  • 优先权号:   CN10359664

▎ 摘  要

NOVELTY - The method comprises preparing graphite oxide and graphene oxide using normal chemical method, taking graphite oxide dispersed into de-ionized water and then ultrasonic dispersing to obtain dispersed precursor solution, where the precursor solution of the graphene oxide is 0.1-0.3mg/ml, and adding ammonium hexafluorotitanate into the solution, uniformly stirring the mixed solution (0.01-0.05mol/L), and placing the solution into a high pressure kettle with polyfluortetraethylene and titanium dioxide/graphene composite nanomaterial at 150-170 degrees C for 4-24 hours. USE - The method is useful for preparing titanium dioxide/graphene composite nanomaterial. ADVANTAGE - The method is capable of simply preparing the titanium dioxide/graphene composite nanomaterial with high yield. DETAILED DESCRIPTION - The method comprises preparing graphite oxide and graphene oxide using normal chemical method, taking graphite oxide dispersed into de-ionized water and then ultrasonic dispersing to obtain dispersed precursor solution, where the precursor solution of the graphene oxide is 0.1-0.3mg/ml, and adding ammonium hexafluorotitanate into the solution, uniformly stirring the mixed solution (0.01-0.05mol/L), placing the solution into a high pressure kettle with polyfluortetraethylene and titanium dioxide/graphene composite nanomaterial at 150-170 degrees C for 4-24 hours, naturally cooling the mixed solution at a room temperature, washing the mixed solution with the de-ionized water, and filtering and vacuum drying the solution to obtain titanium dioxide/graphene composite nanomaterial with crystal surface. An INDEPENDENT CLAIM is included for a titanium dioxide or graphene composite nanomaterial.