• 专利标题:   Preparation of nitrogen doped nano graphene by mixing graphene dispersion solution and nitrogen source solution, magnetically stirring, centrifuging, removing supernatant, drying, adding liquid nitrogen, and microwave heating.
  • 专利号:   CN103818895-A, CN103818895-B
  • 发明人:   ZHANG Y, LI T, LI X, ZHANG X, HUANG J, ZHONG Q
  • 专利权人:   UNIV CHONGQING
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B031/04
  • 专利详细信息:   CN103818895-A 28 May 2014 C01B-031/04 201449 Pages: 8 Chinese
  • 申请详细信息:   CN103818895-A CN10563806 12 Nov 2013
  • 优先权号:   CN10563806

▎ 摘  要

NOVELTY - A nitrogen doped nano graphene is prepared by mixing 1.0-5.0 mg/mL graphene dispersion solution and nitrogen source solution, magnetically stirring for 6-12 hours, centrifuging, removing supernatant, drying at 60 degrees C for 12 hours, adding liquid nitrogen at ratio of 1 g:50 mL, microwave heating at power of 500-1200 W for 5-180 seconds, drying, collecting solid residue, adding 30-200 mL solvent, ultrasonically dispersing for 5-30 minutes, stirring at speed of 2000-6000 revolutions/minute for 10-60 minutes, solid-liquid separating, collecting, and drying at 60-150 degrees C for 30-180 minutes. USE - Method for preparing nitrogen doped nano graphene (claimed). ADVANTAGE - The method is simple and environment-friendly, has convenient operation and low production cost, and reduces production energy consumption. DETAILED DESCRIPTION - A nitrogen doped nano graphene is prepared by mixing 1.0 to 5.0 mg/mL graphene dispersion solution and nitrogen source solution at volume ratio of 1:1-5, magnetically stirring for 6-12 hours, centrifuging, cleaning, removing supernatant, drying at 60 degrees C for 12 hours, adding liquid nitrogen at ratio of 1 g:50 mL, microwave heating at power of 500-1200 W for 5-180 seconds, drying, collecting solid residue, adding 30-200 mL solvent, ultrasonically dispersing for 5-30 minutes, stirring at speed of 2000-6000 revolutions/minute for 10-60 minutes, solid-liquid separating, collecting, and drying at 60-150 degrees C for 30-180 minutes.