• 专利标题:   Catalyst preparation for oxygen reduction reaction of non-noble metal involves adding ferric ammonium citrate solid powder in graphene oxide solution, removing solvent, and placing obtained solid powder in quartz boat for heating.
  • 专利号:   CN104117356-A, CN104117356-B
  • 发明人:   BAO X, TAN D, WANG G, WANG J
  • 专利权人:   CAS DALIAN CHEM PHYSICAL INST, CAS DALIAN CHEM PHYSICAL INST
  • 国际专利分类:   B01J021/18, B01J023/745
  • 专利详细信息:   CN104117356-A 29 Oct 2014 B01J-023/745 201504 Pages: 9 Chinese
  • 申请详细信息:   CN104117356-A CN10148590 26 Apr 2013
  • 优先权号:   CN10148590

▎ 摘  要

NOVELTY - A catalyst is prepared by adding ferric ammonium citrate solid powder in graphene oxide solution, heating or freeze drying to remove solvent to obtain solid powder, a mass ratio of ferric ammonium citrate and graphene oxide solution being 20:1-80:1; placing the solid powder in quartz boat, and putting in tube furnace; introducing inert gas, raising to 600-1000 degrees C, holding for 1 hour, and cooling to room temperature; and treating at 60-100 degrees C for 12-36 hours, filtering, water washing, and baking. USE - Method for preparing catalyst for oxygen reduction reaction of non-noble metal (claimed). ADVANTAGE - The method uses inexpensive precursor, has simple preparation process, and is suitable for large-scale preparation.