• 专利标题:   Graphene powder preparation includes mixing carbon raw material and organic solvent in high temperature high pressure kettle, and heating kettle until the carbon raw material reaches supercritical state of organic solvent.
  • 专利号:   CN102491314-A
  • 发明人:   LIU B, LI L, WANG Q
  • 专利权人:   CHINESE ACAD SCI CHEM INST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102491314-A 13 Jun 2012 C01B-031/04 201280 Pages: 7 Chinese
  • 申请详细信息:   CN102491314-A CN10377170 24 Nov 2011
  • 优先权号:   CN10377170

▎ 摘  要

NOVELTY - A graphene powder is prepared by mixing carbon raw material and organic solvent in high temperature high pressure kettle; heating the kettle until the carbon raw material reaches supercritical state of organic solvent, and keeping for a certain time; releasing pressure of the kettle in short time, receiving the materials in the kettle, and obtaining graphene primary product; and repeatedly cleaning and centrifuging primary product using the organic solvent, further vacuum-drying and obtaining the final graphene powder product. USE - Method for preparation of graphene powder (claimed). ADVANTAGE - The method has mild reaction condition, and is finished in short time. The prepared graphene has large area with preserved crystal structure. DESCRIPTION OF DRAWING(S) - The drawing is a schematic view showing device for preparing graphene powder.