• 专利标题:   Manufacture of graphene involves mixing acid intercalated graphite powder, sulfuric acid and ammonium persulfate, leaving stand, filtering, adding graphite powder into stripper to exfoliate graphene, centrifuging, and freeze-drying.
  • 专利号:   CN106082180-A
  • 发明人:   ZHONG W, WU H
  • 专利权人:   NANTONG WEIDE POWER BATTERY RES INST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106082180-A 09 Nov 2016 C01B-031/04 201702 Pages: 4 Chinese
  • 申请详细信息:   CN106082180-A CN10392613 06 Jun 2016
  • 优先权号:   CN10392613

▎ 摘  要

NOVELTY - The manufacture of graphene involves mixing acid intercalated graphite powder, concentrated sulfuric acid and ammonium persulfate to obtain mixed solution, leaving stand at room temperature for 1-50 days, filtering acid intercalated graphite, adding graphite powder into ultrasonic stripper or high shear stripper to exfoliate graphene, centrifuging to obtain graphene in wet state, and freeze-drying to obtain powdered graphene, where amount of concentrated sulfuric acid and ammonium persulfate is 1-100 times and 1-50 times of the amount of acid intercalated graphite powder. USE - Manufacture of graphene (claimed). ADVANTAGE - The method enables manufacture of graphene with more than 5 layers, intrinsic physical and chemical properties, complete molecular structure and high quality, without graphene oxide component.