• 专利标题:   Iron nitride/nitrogen-doped graphene airgel for oxidation-reduction catalyst comprises iron nitride nanoparticle load and nitrogen-doped graphene airgel.
  • 专利号:   CN103721736-A, CN103721736-B
  • 发明人:   HOU Y, YIN H
  • 专利权人:   UNIV PEKING
  • 国际专利分类:   B01J027/24, H01M004/90
  • 专利详细信息:   CN103721736-A 16 Apr 2014 B01J-027/24 201438 Pages: 11 Chinese
  • 申请详细信息:   CN103721736-A CN10741365 27 Dec 2013
  • 优先权号:   CN10741365

▎ 摘  要

NOVELTY - An iron nitride/nitrogen-doped graphene airgel contains 3-dimensional iron nitride nanoparticle load and nitrogen-doped graphene airgel. USE - Iron nitride/nitrogen-doped graphene airgel for oxidation-reduction catalyst (claimed). ADVANTAGE - The airgel has no noble metal content, low cost, excellent stability and anti-oxidizing methanol property, and catalytic activity exceeding platinum/carbon (Pt/C) catalyst at low amount. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of iron nitride/nitrogen-doped graphene airgel which involves dispersing graphite oxide and organic iron compound in water to obtain oxidized graphite and organic iron compound mixed liquid in which mass ratio graphite oxide:organic iron oxide is 1:0.5-4, adjusting graphite oxide concentration in mixed liquid to 1.5-4 mg/ml, performing hydrothermal reaction at 180-220 degrees C, heat-preserving for 10-14 hours to obtain hydrothermal reaction product, heating to 600-800 degrees C in ammonia gas, and insulating for 1-4 hours. DESCRIPTION OF DRAWING(S) - The drawing shows a high-resolution transmission electron microscope image of iron nitride/nitrogen-doped graphene airgel. (Drawing includes non-English language text).