• 专利标题:   Preparation of large-area graphene sponge by dispersing graphite oxide in solvent, heating substrate, spraying graphene oxide suspension on substrate, carrying out reduction, placing in sealed container filled with hydrazine and heating.
  • 专利号:   CN103086372-A, CN103086372-B
  • 发明人:   WU X, XIE X, BI H, ZHOU Y, XU F, YIN K, SUN L, WAN S
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103086372-A 08 May 2013 C01B-031/04 201373 Pages: 10 Chinese
  • 申请详细信息:   CN103086372-A CN10028166 24 Jan 2013
  • 优先权号:   CN10028166

▎ 摘  要

NOVELTY - Preparation of large-area graphene sponge comprises ultrasonic dispersing graphite oxide in solvent to form 0.1-5 mg/ml graphene oxide suspension, placing substrate on heating platform, adjusting temperature of substrate, spraying graphene oxide suspension using spray gun on substrate, carrying out reduction, placing in sealed container filled with hydrazine, and heating to 75-110 degrees C for 5-48h. USE - Method for preparing large-area graphene sponge (claimed). ADVANTAGE - The sponge has large area and excellent ability to absorb oil and organic solvent. The method is inexpensive, simple and easy to operate.