• 专利标题:   Preparation of molybdenum disulfide/carbon/oxides of iron composite material with three-dimensional structure for lithium ion battery, involves dispersing graphene oxide in deionized water, adding sodium molybdate and thiourea, and stirring.
  • 专利号:   CN114229896-A
  • 发明人:   LIU C, WANG J
  • 专利权人:   GUANGZHOU TWS TECHNOLOGY LTD
  • 国际专利分类:   B82Y030/00, C01B032/05, C01G039/06, C01G049/00, H01M010/0525, H01M004/52, H01M004/58, H01M004/62
  • 专利详细信息:   CN114229896-A 25 Mar 2022 C01G-039/06 202239 Chinese
  • 申请详细信息:   CN114229896-A CN11418385 25 Nov 2021
  • 优先权号:   CN11418385

▎ 摘  要

NOVELTY - Preparation of molybdenum disulfide/carbon/iron oxide composite material with three-dimensional structure involves (a) dispersing graphene oxide in deionized water, adding sodium molybdate and thiourea, and stirring, (b) carrying out hydrothermal reaction on the mixed solution, cooling, filtering, washing, drying and grinding to obtain metal sulfonate/graphene composite powder, (c) ultrasonically dissolving the ferrocene in acetonitrile, then adding metal sulfonate or graphene oxide composite powder for ultrasonic dispersion, (d) transferring the mixture to the microwave for reaction, and (e) calcining the obtained material under the protection of inert gas or nitrogen. USE - Preparation method of molybdenum disulfide/carbon/oxides of iron composite material with three-dimensional structure for lithium ion battery (claimed). ADVANTAGE - The method enables to prepare MoS2/carbon/FeOx composite material with three-dimensional structure, which has high specific capacity and circulation stability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a MoS2/carbon/FeOx composite material of 3D structure.