• 专利标题:   Synthesis of graphene and carbon molecule thin film, involves heating crystal grain of metal catalyst to predetermined temperature under inert gas atmosphere, supplying carbon source gas for predetermined time, and decreasing temperature.
  • 专利号:   JP2012006824-A, JP5563500-B2
  • 发明人:   KANZAKI K, HIBINO H
  • 专利权人:   NIPPON TELEGRAPH TELEPHONE CORP, NIPPON TELEGRAPH TELEPHONE CORP
  • 国际专利分类:   B01J023/755, C01B031/02
  • 专利详细信息:   JP2012006824-A 12 Jan 2012 C01B-031/02 201206 Pages: 19 Japanese
  • 申请详细信息:   JP2012006824-A JP041540 28 Feb 2011
  • 优先权号:   JP122443

▎ 摘  要

NOVELTY - Metal catalyst is heated (S100) to predetermined temperature (A) under inert gas and hydrogen gas atmosphere. The process is maintained for predetermined time, after increasing temperature with respect to predetermined temperature (A). Then, temperature is decreased, to obtain crystal grain of metal catalyst. The obtained metal catalyst is heated to predetermined temperature (B). Carbon source gas is supplied (S110) for predetermined time, after increasing temperature, and temperature is decreased (S120), to obtain graphene and carbon molecule thin film. USE - Synthesis of graphene and carbon molecule thin film. ADVANTAGE - The method economically and easily provides graphene and carbon molecule thin film. DETAILED DESCRIPTION - Metal catalyst is heated to predetermined temperature (A) under inert gas and hydrogen gas atmosphere. The process is maintained for predetermined time, after increasing temperature with respect to predetermined temperature (A). Then, the temperature is decreased at predetermined temperature fall rate, to obtain crystal grain of metal catalyst. The obtained metal catalyst is heated to predetermined temperature (B) under inert gas and hydrogen gas atmosphere. Carbon source gas is supplied for predetermined time, after increasing temperature with respect to predetermined temperature (B), and temperature is decreased at predetermined temperature fall rate, to obtain graphene and carbon molecule thin film. DESCRIPTION OF DRAWING(S) - The drawing shows the flowchart of synthesis of graphene and carbon molecule thin film. (Drawing includes non-English language text) Step for heating metal catalyst (S100) Step for supplying carbon gas source (S110) Step for decreasing temperature (S120)