• 专利标题:   Preparation of blue and purple fluorescent single-layer nitrogen-doped graphene by annealing copper substrate, reducing temperature, heating melamine in furnace to sublimation temperature, and reducing substrate to room temperature.
  • 专利号:   CN108609614-A
  • 发明人:   SHEN Y, ZHENG N, FENG Y, FENG W
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   C01B032/186, C09K011/65
  • 专利详细信息:   CN108609614-A 02 Oct 2018 C01B-032/186 201881 Pages: 7 Chinese
  • 申请详细信息:   CN108609614-A CN10525306 28 May 2018
  • 优先权号:   CN10525306

▎ 摘  要

NOVELTY - Preparation of a blue and purple fluorescent single-layer nitrogen-doped graphene comprises placing melamine in a first temperature zone of a single quartz tube with a tubular furnace, and placing a copper substrate in a second temperature zone of the tubular furnace; annealing the copper substrate under 300 standard cubic centimeter/minute (sccm) argon and 100 sccm hydrogen atmosphere at 1030 degrees C for greater than or equal to 30 minutes; reducing the copper substrate to 900-1000 degrees C, and heating melamine to a sublimation temperature; introducing a mixture of hydrogen, methane, and argon gas at a flow ratio of 20:1:1000; and reducing copper substrate to room temperature. USE - Method for preparing a blue and purple fluorescent single-layer nitrogen-doped graphene. ADVANTAGE - The method achieves uniform and large area blue and purple fluorescent single-layer nitrogen-doped graphene.