• 专利标题:   Preparation of iron oxide conductive polymer graphene ternary absorbing agent used in e.g. electronics, involves mixing graphene oxide thin material and polyethylene glycol, dispersing, adding prepolymer and iron chloride hexahydrate.
  • 专利号:   CN105315964-A, CN105315964-B
  • 发明人:   XUE W, ZHAO R
  • 专利权人:   SICHUAN HUANTAN TECHNOLOGY CO LTD, SICHUAN HUANTAN TECHNOLOGY CO LTD
  • 国际专利分类:   C09K003/00
  • 专利详细信息:   CN105315964-A 10 Feb 2016 C09K-003/00 201648 Pages: 13 English
  • 申请详细信息:   CN105315964-A CN10794927 18 Dec 2014
  • 优先权号:   CN10794927

▎ 摘  要

NOVELTY - Preparation of iron oxide conductive polymer graphene ternary absorbing agent involves mixing flake graphite, concentrated sulfuric acid, concentrated phosphoric acid and potassium permanganate, heating to 40-60 degrees C, stirring for 8-24 hours, adding water and hydrogen peroxide, centrifuging, washing, drying to produce black graphene oxide thin paper-like material, mixing obtained material, ethylene glycol and polyethylene glycol, dispersing, adding a metal phthalocyanine prepolymer and iron chloride hexahydrate, stirring for 1-3 hours, crystallizing, washing, and drying at 80 degrees C. USE - Preparation of iron oxide conductive polymer graphene ternary absorbing agent used in electronics, energy and medical applications. ADVANTAGE - The iron oxide conductive polymer graphene ternary absorbing agent having high conductivity and magnetic characteristics can be produced economically by simple method. DETAILED DESCRIPTION - Preparation of iron oxide conductive polymer graphene ternary absorbing agent involves mixing flake graphite, concentrated sulfuric acid, concentrated phosphoric acid and potassium permanganate in ratio of 1 g:90-150 mL:10-18 mL:3-10 g, stirring at room temperature for 1-3 hours, heating to 40-60 degrees C, stirring for 8-24 hours, adding deionized water and hydrogen peroxide, centrifuging to produce yellow precipitate, washing with deionized water and dilute hydrochloric acid, drying at 40-60 degrees C for 24-48 hours to produce black graphene oxide thin paper-like material, mixing obtained material, ethylene glycol and polyethylene glycol, ultrasonically dispersing, adding a metal phthalocyanine prepolymer and iron chloride hexahydrate, stirring for 1-3 hours, crystallizing, washing with deionized water and ethanol, and drying at 80 degrees C.