• 专利标题:   Preparing graphene oxide/epoxy resin composite material modified by chitosan-polyethylene glycol diglycidyl ether used in e.g. aerospace, military industry, and electronic packaging, comprises dissolving chitosan powder in acetic acid solution and stirring, heating and curing.
  • 专利号:   CN114479356-A
  • 发明人:   MA R, SONG Y, ZHU S, ZHANG W, MA L
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   C08G081/00, C08L063/00, C08L087/00
  • 专利详细信息:   CN114479356-A 13 May 2022 C08L-063/00 202264 Chinese
  • 申请详细信息:   CN114479356-A CN10276520 21 Mar 2022
  • 优先权号:   CN10276520

▎ 摘  要

NOVELTY - Preparing graphene oxide/epoxy resin composite material modified by chitosan-polyethylene glycol diglycidyl ether comprises (i) dissolving chitosan powder in acetic acid solution and stirring to obtain chitosan solution, ultrasonically dispersing the graphene oxide powder in deionized water to obtain a graphene oxide dispersion, mixing the chitosan solution and the graphene oxide dispersion, and stirring to obtain the reaction solution I, washing the reaction solution I, and freeze-drying to obtain graphene oxide-chitosan hybrid material, (ii) preparing graphene oxide-chitosan-polyethylene glycol diglycidyl ether hybrid material, and (iii) adding the graphene oxide-chitosan-polyethylene glycol diglycidyl ether hybrid material into acetone, and ultrasonically dispersing, heating and curing to obtain a graphene oxide-chitosan-polyethylene glycol diglycidyl ether/epoxy resin composite material. USE - The composite material is used in aerospace, military industry, biological medicine, sports device, and electronic packaging. ADVANTAGE - The method: avoids the problem of weak interface intensity between the graphene and the epoxy resin; and has enhancing effect than pure oxidation graphene. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a kind of chitosan-polyethylene glycol diglycidyl ether modified oxidized graphene/epoxy resin composite material.