• 专利标题:   Preparation of three-dimensional graphene-loaded nano palladium catalyst by soft template used for reducing nitrobenzene to aniline includes weighing graphite oxide, treating, adding palladium chloride aqueous solution, mixing and drying.
  • 专利号:   CN108295843-A
  • 发明人:   LIU P, CHEN Y, ZHANG Z, LI Y
  • 专利权人:   UNIV CHANGZHOU
  • 国际专利分类:   B01J023/44, B01J037/16, B01J037/34, C07C209/36, C07C211/46
  • 专利详细信息:   CN108295843-A 20 Jul 2018 B01J-023/44 201856 Pages: 7 Chinese
  • 申请详细信息:   CN108295843-A CN10052031 19 Jan 2018
  • 优先权号:   CN10052031

▎ 摘  要

NOVELTY - Preparation of three-dimensional graphene-loaded nano palladium catalyst by soft template comprises weighing 0.5-4 mg/ml graphite oxide, adding deionized water in an emulsion system of ethanol and cyclohexane, sonicating for 5-20 minutes at room temperature to obtain dispersed graphene oxide emulsion, adding 60-100 mg ascorbic acid to emulsion, treating mixture in water bath at 60-90 degrees C for 0.25-2 hours, adding 0.3-1 mL palladium chloride aqueous solution, mixing in oil bath, centrifuging mixture with deionized water, washing ethanol and drying. USE - Method of preparing three-dimensional graphene-loaded nano palladium catalyst by soft template used for reducing nitrobenzene to aniline (claimed). ADVANTAGE - The catalyst exhibits high catalytic activity and stability and has high recovery rate, mild preparation condition, simple process and low cost.