• 专利标题:   Preparing polyacrylamide gel with controllable pore size, by mixing graphene oxide, acrylic acid, thionyl chloride, hydroquinone and triethylamine, synthesizing, dissolving acrylic functionalized graphene in dimethylformamide and mixing functionalized graphene in e.g. dimethylformamide solution.
  • 专利号:   CN113358875-A
  • 发明人:   DING X, XIE H, ZHANG T, GUO W
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   G01N033/68, G01N033/531, G01N021/33, G01N021/35
  • 专利详细信息:   CN113358875-A 07 Sep 2021 G01N-033/68 202192 Pages: 11 Chinese
  • 申请详细信息:   CN113358875-A CN10441094 23 Apr 2021
  • 优先权号:   CN10441094

▎ 摘  要

NOVELTY - Method for preparing polyacrylamide gel with a controllable pore size, involves mixing graphene oxide, acrylic acid, thionyl chloride, hydroquinone and triethylamine, synthesizing under a protective gas atmosphere to obtain acrylic functionalized graphene, dissolving the acrylic functionalized graphene in dimethylformamide to obtain a dimethylformamide solution of functionalized graphene, and mixing functionalized graphene in dimethylformamide solution, acrylamide, N-isopropylacrylamide aqueous solution, tris(hydroxymethyl)aminomethane (Tris) hydrochloride, sodium dodecyl sulfate (SDS), Triton X-100 (RTM: t-octyl phenoxy polyethoxy ethanol), photosensitive compound MAP-mPyTC, ammonium persulfate (APS) and tetramethylethylenediamine (TEMED) gel under anaerobic conditions. USE - The method is useful for preparing polyacrylamide gel with controllable pore size (claimed). ADVANTAGE - The method provides reversible adjustment of the gel size, and short required change time. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for polyacrylamide gel with controllable pore size, which is prepared by the method.