• 专利标题:   Preparing tin sulfide-graphene oxide composite photocatalyst for visible-light photocatalytic degradation of organic contaminants, by mixing stannous chloride dihydrate, water and ethylene glycol and mixing with graphene oxide solution.
  • 专利号:   CN106622292-A, CN106622292-B
  • 发明人:   ZHU L, ZHANG Q, WANG B, FAN Y, MENG Q, FAN L
  • 专利权人:   YANCHENG INST TECHNOLOGY, YANCHENG INST TECHNOLOGY
  • 国际专利分类:   B01J027/04, C02F001/30, C02F101/38
  • 专利详细信息:   CN106622292-A 10 May 2017 B01J-027/04 201744 Pages: 16 Chinese
  • 申请详细信息:   CN106622292-A CN11190260 20 Dec 2016
  • 优先权号:   CN11190260

▎ 摘  要

NOVELTY - Preparation method of tin sulfide-graphene oxide composite photocatalyst involves (a) mixing stannous chloride dihydrate, water and ethylene glycol, (b) mixing mixed solution (I) with graphene oxide solution, (c) mixing mixed solution (II) with polyvinylpyrrolidone and sodium thiosulfate, (d) adjusting pH of the mixed solution (III) to 7.5-9, alternately heating the mixed solution (III) under microwave conditions at a powder of 800 W for 3-5 minutes at an interval of 8-12 seconds, and (e) washing, centrifuging and drying the obtained material. USE - Method is useful for preparing tin sulfide-graphene oxide composite photocatalyst, which is useful for visible-light photocatalytic degradation of organic contaminants (all claimed). DETAILED DESCRIPTION - Preparation method of tin sulfide-graphene oxide composite photocatalyst involves (a) mixing stannous chloride dihydrate, water and ethylene glycol to obtain mixed solution (I), (b) mixing mixed solution (I) with graphene oxide solution to obtain mixed solution (II), (c) mixing mixed solution (II) with polyvinylpyrrolidone and sodium thiosulfate to obtain mixed solution (III), (d) adjusting pH of the mixed solution (III) to 7.5-9, alternately heating the mixed solution (III) under microwave condition at a powder of 800 W for 3-5 minutes at an interval of 8-12 seconds, and (e) washing, centrifuging and drying the obtained material. An INDEPENDENT CLAIM is included for tin sulfide-graphene oxide composite photocatalyst prepared by the above method.