• 专利标题:   Manufacture of mesoporous material involves diluting 1-hexadecyl-3-methylimidazolium chloride in deionized water, adding ethyl alcohol, ammonium hydroxide, niobium, graphene, and tetraethyl orthosilicate, stirring, filtering, washing and drying.
  • 专利号:   BR102022010583-A2
  • 发明人:   FINKLER D E, DE OLIVEIRA PEREIRA F, MIGNONI M L, TODERO A S, DALLAGO R M
  • 专利权人:   FINKLER D E
  • 国际专利分类:   B01J029/00
  • 专利详细信息:   BR102022010583-A2 06 Sep 2022 B01J-029/00 202301 Pages: 21
  • 申请详细信息:   BR102022010583-A2 BR10010583 31 May 2022
  • 优先权号:   BR10010583

▎ 摘  要

NOVELTY - Manufacture of mesoporous material using niobium doped grpahenosilicate possessing MCM topology involves (i) diluting 2.4 g 1-hexadecyl-3-methylimidazolium chloride in 50 mL deionized water under magnetic stirring, (ii) adding 50 mL ethyl alcohol and 10 mL ammonium hydroxide, (iii) solubilizing the variable amount of niobium obtain the silicon and niobium molar ratio of 1-10, (iv) adding 0.17 g graphene, (v) stirring for 10 minutes, (vi) adding 3.4 g tetraethyl orthosilicate, and magnetic stirring at 25-200 rpm for 2 hours at 23-25° C, (vii) filtering and washing with 50 mL deionized water for 3 times, and (viii) drying in an oven at 100° C until constant weight. USE - Manufacture of mesoporous material. ADVANTAGE - The method is carried out in room temperature, and produces mesoporous material using ionic solid which is easily synthesized.