• 专利标题:   Preparing carbon nitride-graphene composite material used in adsorption treatment of rare earth elements in water comprises adding multilayer graphene oxide to carbon-nitrogen precursor solution, dispersing and carrying out pyrolysis reaction of carbon nitride-graphene pyrolysis precursor material.
  • 专利号:   CN113457621-A
  • 发明人:   YANG C, XU H, HE Y, HE J, FU C
  • 专利权人:   UNIV SHAOXING
  • 国际专利分类:   C02F101/20, C02F001/30, B01J020/30, C02F001/28, B01J027/24, B01J020/02, B01J020/20
  • 专利详细信息:   CN113457621-A 01 Oct 2021 B01J-020/20 202103 Chinese
  • 申请详细信息:   CN113457621-A CN10575773 26 May 2021
  • 优先权号:   CN10575773

▎ 摘  要

NOVELTY - Preparing carbon nitride-graphene composite material comprises (1) dissolving proper amount of carbon and nitrogen precursor in proper amount of water to prepare a carbon and nitrogen precursor solution, (2) adding proper amount of multilayer graphene oxide into the carbon-nitrogen precursor solution, and dispersing mixture by ultrasonic vibration and stirring, (3) reacting the mixed solution at 50-150degrees Celsius for at least 30 minutes, (4) sequentially centrifuging, filtering and drying the solution after completion of the reaction to obtain a carbon nitride-graphene pyrolysis precursor material, (5) placing carbon nitride-graphene pyrolysis precursor material in a microwave reactor, and rapidly increasing the temperature to 750-1200degrees Celsius for pyrolysis reaction under anoxic or anaerobic conditions, and (6) grinding the pyrolysis reaction product to obtain a finished product. USE - The carbon nitride-graphene composite material is useful in adsorption treatment of rare earth elements in water (claimed). ADVANTAGE - The composite material has simple process, larger specific surface area and better adsorption effect and is economical.