• 专利标题:   Making composite material used in lithium battery, by mixing dimethylformamide and water, adding expanded graphite, oscillating and adding manganese acetate tetrahydrate and ferrous chloride tetrahydrate to multilayer graphene solution.
  • 专利号:   CN108365182-A
  • 发明人:   XU J, WU F, HU X, SONG K, WU J, GAO H, YAO Y, LIAO K, HAN Z
  • 专利权人:   UNIV HANGZHOU DIANZI
  • 国际专利分类:   H01M004/36, H01M004/50, H01M004/62, H01M010/052
  • 专利详细信息:   CN108365182-A 03 Aug 2018 H01M-004/36 201861 Pages: 12 Chinese
  • 申请详细信息:   CN108365182-A CN11456784 28 Dec 2017
  • 优先权号:   CN11456784

▎ 摘  要

NOVELTY - The method for preparing iron ion-doped tetramanganese tetroxide/multilayer graphene composite material involves (a) mixing dimethylformamide and distilled water in a volume ratio of 8:2 as a mixed solvent, (b) adding expanded graphite and ultrasonically oscillating for 2-5 hours to obtain a multilayer graphene mixed solution, (c) adding manganese acetate tetrahydrate and ferrous chloride tetrahydrate to multilayer graphene mixed solution, stirring at 30 degrees C for 5-10 minutes, pouring the solution into a hydrothermal reactor, hydrothermally reacting at 100-130 degrees C for 2-5 hours and cooling to room temperature, and (d) taking out reactants, washing with alcohol and distilled water 3-5 times and then dried in a drying oven at 60 degrees C for 24 hours to obtain the composite material. USE - Method is useful for preparing iron ion-doped tetramanganese tetroxide/multilayer graphene composite material, which is useful as a cathode material for lithium battery (all claimed). ADVANTAGE - The composite material has excellent electrochemical performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for iron ion-doped tetramanganese tetroxide/multilayer graphene composite material prepared by the above method.