• 专利标题:   Preparing microorganism-loaded graphene aerogel metal organic framework composite material useful for azo dye treatment, comprises mixing graphene oxide solution and ascorbic acid, reacting, freeze-drying and subjecting to thermal annealing.
  • 专利号:   CN108821445-A
  • 发明人:   LU J, CHEN D, JIANG J
  • 专利权人:   UNIV SOOCHOW
  • 国际专利分类:   C02F003/34, C02F001/28, C02F101/30, C02F101/38
  • 专利详细信息:   CN108821445-A 16 Nov 2018 C02F-003/34 201903 Pages: 12 Chinese
  • 申请详细信息:   CN108821445-A CN10547796 31 May 2018
  • 优先权号:   CN10547796

▎ 摘  要

NOVELTY - Preparing microorganism-loaded graphene aerogel metal organic framework composite material comprises: (i) mixing the graphene oxide solution and ascorbic acid, reacting under boiling water bath environment, ice bath environment, room temperature environment and boiling water bath environment, freeze-drying and subjecting to thermal annealing treatment to obtain graphene aerogel; (ii) immersing the graphene aerogel in silane coupling agent solution and terephthalic acid solution to obtain carboxylated graphene aerogel; (iii) self-assembling the ferric chloride ethanol solution and trimesic acid ethanol solution, then self-assembling the carboxylated graphene aerogel through layers to obtain graphene aerogel metal organic framework composite material; and (iv) loading the microorganism on the surface of graphene aerogel metal organic framework composite. USE - The microorganism-loaded graphene aerogel metal organic framework composite material is useful for azo dye treatment (claimed). ADVANTAGE - The azo dye has good absorbing and degrading effect. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) processing azo dye, comprising preparing microorganism-loaded graphene aerogel metal organic framework composite material, adding azo dye solution into the microentrained graphene aerogel metal organic framework composite material; and (2) carboxylated graphene aerogel.