• 专利标题:   Preparation of graphene for lithium batteries, involves heating sodium chloride and calcium chloride salt, forming composite molten salt, adding expanded graphite, grinding graphite and salt embedded large particles, dispersant and ethanol, stripping, filtering, desalting and drying.
  • 专利号:   CN113428852-A
  • 发明人:   LI J, SI W, ZENG J, CHEN Q
  • 专利权人:   CHENGDU NEW KELI CHEM ENG SCI TECHNIC
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN113428852-A 24 Sep 2021 C01B-032/19 202102 Chinese
  • 申请详细信息:   CN113428852-A CN10777396 09 Jul 2021
  • 优先权号:   CN10777396

▎ 摘  要

NOVELTY - Preparation of graphene, involves (S1) uniformly mixing sodium chloride and calcium chloride salt, heating and melting to form composite molten salt, adding expanded graphite, stirring and dispersing uniformly, embedding surface and interlayer of molten salt and expanded graphite to form whole mass, cooling, crushing to obtain graphite and salt embedded large particles, (S2) grinding along with dispersant, ethanol and grinding medium for 3-5 hours in ball mill, and stripping embedded graphite to form graphene, (S3) filtering grinded material by coarse screen, removing grinding medium, fine screen filtering, removing ethanol, desalting by repeatedly washing and drying. USE - Preparation of graphene for high-end products e.g. lithium batteries, heat dissipation coatings and printed conductive pastes. ADVANTAGE - The method improves grinding efficiency and obtains high-quality graphene.