• 专利标题:   Producing textile fibers based on graphene oxide and polyester involves providing load of polyester particles, and then providing dispersion charge of graphene oxide particles in suitable solvent.
  • 专利号:   WO2021097544-A1, BR102019024477-A2
  • 发明人:   FECHINE G J M, MUNOZ P A R, ANDRADE R J E, LAMBERT T D O, DINI C R, MACEDO FECHINE G J, ESPANHOL ANDRADE R J, DE OLIVEIRA LAMBERT T, ROGERIO DINI C
  • 专利权人:   DINI TEXTIL IND COMERCIO LTDA, INST PRESBITERIANO MACKENZIE
  • 国际专利分类:   D01D001/02, D01D001/04, D01F001/02, D01F001/09, D01F001/10, B29C048/92, D01D005/088, D01F006/62
  • 专利详细信息:   WO2021097544-A1 27 May 2021 D01F-001/02 202149 Pages: 21
  • 申请详细信息:   WO2021097544-A1 WOBR050483 18 Nov 2020
  • 优先权号:   BR10024477

▎ 摘  要

NOVELTY - Producing textile fibers based on graphene oxide and polyester involves providing a load of polyester particles smaller than 1 mm, and then providing dispersion charge of graphene oxide particles with a thickness of 1-10 nm and a lateral dimension of 0.5-10 micrometers in a suitable solvent and with a concentration of 1.0-5.0 g/l. The graphene oxide dispersion charge is pre-mixed with the polyester particle charge with the graphene oxide concentration varying as a function of the final properties of the polymeric nanocomposite to be obtained. The premix of the polyester filler and the graphene oxide dispersion filler is dried at 50 degrees C under vacuum and under constant agitation for forming a heterogeneous hybrid compound containing polyester granules covered with oxide sheets of graphene. The heterogeneous hybrid compound is subjected to a final drying to a moisture content of 20000-30000 parts per million. USE - Method for producing textile fibers based on graphene oxide and polyester for textile industry. ADVANTAGE - The method produces the textile fibers in a simple, cost-effective and eco-friendly manner with excellent distribution in the polyester matrix without clumps and allowing the use of the threads for various applications including fabric production. DETAILED DESCRIPTION - Producing textile fibers based on graphene oxide and polyester involves providing a load of polyester particles smaller than 1 mm, and then providing dispersion charge of graphene oxide particles with a thickness of 1-10 nm and a lateral dimension of 0.5-10 micrometers in a suitable solvent and with a concentration of 1.0-5.0 g/l. The graphene oxide dispersion charge is pre-mixed with the polyester particle charge with the graphene oxide concentration varying as a function of the final properties of the polymeric nanocomposite to be obtained. The premix of the polyester filler and the graphene oxide dispersion filler is dried at 50 degrees C under vacuum and under constant agitation for forming a heterogeneous hybrid compound containing polyester granules covered with oxide sheets of graphene. The heterogeneous hybrid compound is subjected to a final drying to a moisture content of 20000-30000 parts per million. The heterogeneous hybrid compound is submitted to mixing in the molten state in a twin screw extruder for forming a polymeric nanocomposite. The polymeric nanocomposite is collected and submitted to drying silos. The polymeric nanocomposite is processed in an extruder for yarn production. DESCRIPTION OF DRAWING(S) - The drawing shows a graphical representation depicting distribution of graphene oxide particles generated from X-ray microtomography images of the polyester nanocomposite and graphene oxide.