• 专利标题:   Producing expanded graphite used for producing high purity graphene, comprises mixing graphite with acid to perform acid treatment, introducing expansion agent including sulfur oxoacid and metal halide, and expanding by applying microwaves.
  • 专利号:   KR2019096074-A, KR2028911-B1
  • 发明人:   LEE S S, AN K, LIM J, MYUNG S, SEOG S, LEE Y B
  • 专利权人:   KOREA RES INST CHEM TECHNOLOGY
  • 国际专利分类:   C01B032/184, C01B032/198, C01B032/225, C01B032/23
  • 专利详细信息:   KR2019096074-A 19 Aug 2019 C01B-032/225 201972 Pages: 9
  • 申请详细信息:   KR2019096074-A KR015573 08 Feb 2018
  • 优先权号:   KR015573

▎ 摘  要

NOVELTY - Producing expanded graphite, comprises (a) mixing graphite with acid to perform acid treatment, (b) introducing expansion agent including sulfur oxoacid and metal halide, and (c) expanding by applying microwaves. USE - The expanded graphite is useful in producing high purity graphene (claimed). ADVANTAGE - The method produces expanded graphite with low energy using sulfur oxoacid compound and metal halide. The expanded graphite can be expanded at high expansion rate even with low energy, and produces high purity graphene. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for producing graphene, comprising (i) preparing graphene oxide by oxidizing the expanded graphite prepared by the above method, and (ii) reducing the graphene oxide.