• 专利标题:   Preparing composite modified expand graphene used in printing-dyeing waste water treatment comprises e.g. soaking crystalline flake graphite in cetyltrimethylammonium bromide-potassium bromide composite modifier solution, washing, expanding.
  • 专利号:   CN104888707-A
  • 发明人:   FAN P, JIAO C, LIN A, SUN Y, WANG H, XU C
  • 专利权人:   UNIV BEIJING CHEM TECHNOLOGY
  • 国际专利分类:   B01J020/20, B01J020/30, C02F001/28
  • 专利详细信息:   CN104888707-A 09 Sep 2015 B01J-020/20 201580 Pages: 6 Chinese
  • 申请详细信息:   CN104888707-A CN10318607 11 Jun 2015
  • 优先权号:   CN10318607

▎ 摘  要

NOVELTY - Preparing composite modified expand graphene, comprises taking quantitative natural crystalline flake graphite as raw material for expandable graphite preparation at a certain temperature, soaking in cetyltrimethylammonium bromide-potassium bromide composite modifier solution, water washing, drying, expanding to obtain composite modified expand graphene, cetyltrimethylammonium bromide, potassium bromide concentration is 0.02-0.12 mol/l, 0.05-0.2 mol/l, the solvent is alcohol, and water, the ratio of expandable graphite and solution is 1:0.1-1:0.5. USE - The composite modified expand graphene is used in printing and dyeing waste water treatment, and printing and dyeing static adsorption (claimed), and printing and dyeing wastewater purification. ADVANTAGE - The method realizes low expansion temperature, and saves energy. The composite modified expand graphene has increased surface active sites, is loaded with rich surface functional groups, and can absorb variety of dyes. DETAILED DESCRIPTION - Preparing composite modified expand graphene, comprises taking quantitative natural crystalline flake graphite as raw material for expandable graphite preparation at a certain temperature, soaking in cetyltrimethylammonium bromide-potassium bromide composite modifier solution, water washing, drying, expanding to obtain composite modified expand graphene, cetyltrimethylammonium bromide, potassium bromide concentration is 0.02-0.12 mol/l, 0.05-0.2 mol/l, the solvent is alcohol, and water, the ratio of expandable graphite and solution is 1:0.1-1:0.5, the soaking temperature is 30-80 degrees C, soaking time is 5-8 hours, expanding device is low temperature furnace and muffle furnace.