• 专利标题:   2-mercaptobenzothiazole modified graphene oxide used for anti-corrosive coating, comprises matrix resin, flatting agent, de-foaming agent, dispersant, auxiliary agent, and diluent.
  • 专利号:   CN106700823-A, WO2018095364-A1, CN106700823-B
  • 发明人:   DAI L, WANG S, SHAO Z, CHEN T, YUAN C, ZENG B, XU Y, LUO W
  • 专利权人:   UNIV XIAMEN, UNIV XIAMEN
  • 国际专利分类:   C09D127/12, C09D133/00, C09D161/20, C09D163/00, C09D167/00, C09D167/08, C09D175/04, C09D005/08, C09D007/12, C09D007/62
  • 专利详细信息:   CN106700823-A 24 May 2017 C09D-163/00 201747 Pages: 7 Chinese
  • 申请详细信息:   CN106700823-A CN11036205 23 Nov 2016
  • 优先权号:   CN11036205

▎ 摘  要

NOVELTY - 2-mercaptobenzothiazole modified graphene oxide (I) comprises 5-20 pts. wt. matrix resin, 30-70 pts. wt. flatting agent, 0.5-1.0 pts. wt. de-foaming agent, 0.5-1.0 dispersant, 0.5-1.0 pts. wt. auxiliary agent, and 20-35pts. wt. diluent. USE - 2-mercaptobenzothiazole modified graphene oxide used for anti-corrosive coating (claimed). ADVANTAGE - The 2-mercaptobenzothiazole modified graphene oxide has improved dispersibility, mechanical effect and corrosion resistance. DETAILED DESCRIPTION - 2-mercaptobenzothiazole modified graphene of formula (I).. An INDEPENDENT CLAIM is included for a method for preparing 2-mercaptobenzothiazole modified graphene oxide, which involves: (A) taking amount of graphene oxide, cyanuric chloride, sodium bicarbonate in the flask having mass ratio of 1-30g:1-8mol:1-20mol, and 100-2000ml N, N-dimethyl, mixing and stirring at 50 degrees C for 10-24 hours, cooling and filtering to obtain a precipitate; (B) mixing the obtained precipitate with 1,2-mercaptobenzothiazole, potassium hydroxide in mass ratio of 1-30 g:1-8mol in the flask, and adding 100-2000 ml acetone to disperse, as reaction is carried out for 6-10 hours, cooling and filtering to obtain filtrate; and (C) mixing rest components into obtained filtrate for 1-4 hour and filtering to obtain desired product.