• 专利标题:   Preparing modified graphene and nano-cellulose composite temperature-sensitive material involves dissolving graphene in absolute ethanol, adding ammonia water rapidly under magnetic stirring, and continuously stirring.
  • 专利号:   CN107226923-A
  • 发明人:   HU C
  • 专利权人:   ANHUI YINGSHANG ZHENGTAI ELECTRIC APPLIA
  • 国际专利分类:   C08B015/06, C08J009/28, C08K003/04, C08K009/02, C08K009/04, C08L001/08
  • 专利详细信息:   CN107226923-A 03 Oct 2017 C08J-009/28 201781 Pages: 4 Chinese
  • 申请详细信息:   CN107226923-A CN10438095 12 Jun 2017
  • 优先权号:   CN10438095

▎ 摘  要

NOVELTY - Preparing modified graphene and nano-cellulose composite temperature-sensitive material involves dissolving 20-30 pts. wt. graphene in 100-200 pts. wt. absolute ethanol, adding 2-5 pts. wt. ammonia water rapidly under magnetic stirring, continuously stirring, adding 1-2 pts. wt. decahexaalkyl trimethyl ammonium bromide first dissolving in anhydrous ethanol, adding solution in dropwise manner with rapid stirring, maintaining at 60-80 degrees C, magnetic stirring for 2-5 hours. USE - Method for preparing modified graphene and nano-cellulose composite temperature-sensitive material (claimed). ADVANTAGE - The method enables to prepare modified graphene and nano-cellulose composite temperature-sensitive material in simple manner, cost-effective, which has avoids raw material graphite agglomeration, and has excellent mechanical property. DETAILED DESCRIPTION - Preparing modified graphene and nano-cellulose composite temperature-sensitive material involves dissolving 20-30 pts. wt. graphene in 100-200 pts. wt. absolute ethanol, adding 2-5 pts. wt. ammonia water rapidly under magnetic stirring, continuously stirring, adding 1-2 pts. wt. decahexaalkyl trimethyl ammonium bromide first dissolving in anhydrous ethanol, adding solution in dropwise manner with rapid stirring, maintaining at 60-80 degrees C, magnetic stirring for 2-5 hours, and standing. 0.5-1 pts. wt. nanocellulose is dissolved into 100-150 pts. wt. water, added 0.5-1.5 pts. wt. alkyl phenol polyoxyethylene ether, 2-10 pts. wt. urea, low temperature ultrasonic dispersing, magnetic stirring for 1- 12 hours at 20-30 degrees C, and placing for 2-3 days, and standing. The solution obtain is heated in a water bath at 35-55 degrees C, added 1-2 pts. wt. precursor solution under stirring, kept temperature for 40-60 minutes, added product obtained, maintained temperature, stirred for 10-12 hours, removed cetyltrimethylammonium bromide, centrifuged by using distilled water and alcohol for 3-4 times, and freeze-dried to obtain final product.