• 专利标题:   GRAPHENE-BASED NANOSTRUCTURED TWO DIMENSIONAL FILMS AND PROCESS FOR PREPARING THE SAME.
  • 专利号:   RO132432-A2
  • 发明人:   ATHANASIOS T, BALAN A E, CUCU A, STAMATIN I
  • 专利权人:   UNIV DIN BUCURESTI
  • 国际专利分类:   B82Y030/00, C01B031/02
  • 专利详细信息:   RO132432-A2 30 Mar 2018 C01B-031/02 201823 Pages: 0 English
  • 申请详细信息:   RO132432-A2 RO000662 21 Sep 2016
  • 优先权号:   RO000662

▎ 摘  要

NOVELTY - The invention relates to a graphene-based nanostructured bidimensional film and to the process for preparing the same. According to the invention, the film exhibits layers the surfaces of which are made of hexagonal lattices interconnected by polyhedral channels of 1 um, as well as of smaller lattices, with electric conductivity of 0.003...0.016 S/cm, thermal stability of 900...1000 degrees C, hydrophobic character with a static contact angle value ranging from 21...151 degrees . The process for preparing the film, as claimed by the invention, consists in applying a polyimide laser pyrolysis method, while monitoring and varying three parameters: laser power, scanning rate and operation step interval, resulting in five types of products, the laser pyrolysis being conducted as intermittent and overlapping steps, to create either zones surface-graphitized by thermal diffusion, or consecutive thin strips which receive an increasingly high level of laser fluence, at a laser power in the range of 4.8...6W, with a scanning rate of 20...450 mm/s, an interval between the steps of 10...120 um, with base fluence in the range of 0.27...4.8 J/mm-2 and maximum reached fluence of 0.59...9.60 J/mm-2.