• 专利标题:   Graphene quantum dot-sulfide composite material preparation performing ultrasonic dispersion of graphene oxide with deionized water to obtain brown-yellow suspension, and adding zinc acetate and thiourea to brown-yellow suspension.
  • 专利号:   CN103983672-A
  • 发明人:   JIANG K, XU F, BAI D, GAO Z, WANG J, WU D
  • 专利权人:   UNIV HENAN NORMAL
  • 国际专利分类:   B82Y030/00, C01B031/04, C01G011/02, C01G009/08, G01N027/26
  • 专利详细信息:   CN103983672-A 13 Aug 2014 G01N-027/26 201471 Pages: 10 Chinese
  • 申请详细信息:   CN103983672-A CN10215152 21 May 2014
  • 优先权号:   CN10215152

▎ 摘  要

NOVELTY - Graphene quantum dot-sulfide composite material preparation performing ultrasonic dispersion of graphene oxide (2-8mg) with deionized water (70mL) to obtain a brown-yellow suspension, and adding zinc acetate (0.266g) or cadmium acetate (0.123g) and thiourea (0.228g) to the brown-yellow suspension to obtain a mixture. Polyacrylic acid (5mL) is added to the mixture, and then ammonium hydroxide is added to the mixture to adjust pH value to 8-10. USE - Method for preparing graphene quantum dot-sulfide composite material (claimed). ADVANTAGE - The method enables preparing graphene quantum dot-sulfide composite material in a cost-effective and eco-friendly manner. DETAILED DESCRIPTION - Graphene quantum dot-sulfide composite material preparation performing ultrasonic dispersion of graphene oxide (2-8mg) with deionized water (70mL) to obtain a brown-yellow suspension, and adding zinc acetate (0.266g) or cadmium acetate (0.123g) and thiourea (0.228g) to the brown-yellow suspension to obtain a mixture. Polyacrylic acid (5mL) is added to the mixture, and then ammonium hydroxide is added to the mixture to adjust pH value to 8-10. The product is entered into a hydro-thermal reaction kettle for performing hydro-thermal reaction at 160-200 degrees C for 6-8h minutes to obtain black precipitate. The black precipitate is washed, and then dried graphene quantum dot-sulfide composite material.