• 专利标题:   Preparation of nitrogen-doped graphene involves adding graphene oxide and surfactant in ether solvent, stirring, volatilizing solvent, placing in inert gas and ammonia gas mixture, heating, and cooling.
  • 专利号:   CN103359708-A, CN103359708-B
  • 发明人:   WANG Y, ZHONG H, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B031/04
  • 专利详细信息:   CN103359708-A 23 Oct 2013 C01B-031/04 201412 Pages: 9 Chinese
  • 申请详细信息:   CN103359708-A CN10084427 27 Mar 2012
  • 优先权号:   CN10084427

▎ 摘  要

NOVELTY - Preparation of nitrogen-doped graphene involves dispersing graphite oxide in deionized water; carrying out ultrasonic treatment; filtering; drying to obtain graphene oxide; adding graphene oxide and Pluronic F-127 (RTM: Non-ionic copolymer surfactant) in ether solvent; stirring for 2-4 hours; volatilizing solvent to obtain graphene oxide/Pluronic F-127 (RTM: Non-ionic copolymer surfactant) mixture; placing mixture in inert gas and ammonia gas mixture; heating at 5-20 degrees C/minute at 800-1000 degrees C for 30-120 minutes; and cooling at room temperature. USE - Preparation of nitrogen-doped graphene. ADVANTAGE - The method produces nitrogen-doped graphene with smaller particle size. It has simple oxidation step and device requirement, convenient operation, and suitable for large scale industrial production. DETAILED DESCRIPTION - Preparation of nitrogen-doped graphene comprises dispersing graphite oxide in deionized water; carrying out ultrasonic treatment; filtering; drying to obtain graphene oxide; adding graphene oxide and Pluronic F-127 (RTM: Non-ionic copolymer surfactant) in ether solvent; stirring for 2-4 hours; volatilizing solvent to obtain graphene oxide/Pluronic F-127 (RTM: Non-ionic copolymer surfactant) mixture; placing mixture in mixed gas atmosphere consisting of inert gas and ammonia gas; heating at 5-20 degrees C/minute at 800-1000 degrees C for 30-120 minutes; and cooling at room temperature to obtain nitrogen-doped graphene. DESCRIPTION OF DRAWING(S) - The drawing shows a block diagram of a process for preparing nitrogen-doped graphene (Drawing includes non-English language text).