• 专利标题:   Production of porous material, by obtaining graphene quantum dot (GQD) powder, dissolving in dimethylformamide solution to obtain GQD-functionalized monomer, adding polyvinyl alcohol and hydroquinone, polymerizing and drying.
  • 专利号:   CN107473211-A
  • 发明人:   LIU Y, DI D
  • 专利权人:   LANZHOU CHEM PHYSICS INST CHINESE ACAD
  • 国际专利分类:   C01B032/194, C08F220/56, C08L029/04
  • 专利详细信息:   CN107473211-A 15 Dec 2017 C01B-032/194 201807 Pages: 10 Chinese
  • 申请详细信息:   CN107473211-A CN10639929 31 Jul 2017
  • 优先权号:   CN10639929

▎ 摘  要

NOVELTY - Production of porous material involves heating citric acid, adding sodium hydroxide solution, dialyzing, filtering, dialyzing filtrate, freeze-drying to obtain brown-yellow graphene quantum dot (GQD) powder, dissolving powder in dimethylformamide solution, adding solution of thionyl chloride to obtain chlorinated GQD, centrifuging, washing, heating, centrifuging, lyophilizing to obtain GQD-functionalized monomer, adding deionized water, polyvinyl alcohol and hydroquinone to obtain dispersed phase, stirring, heating, filtering, polymerizing, washing and drying. USE - Production of porous material (claimed). ADVANTAGE - The method enables simple production of porous material with high mechanical strength. DETAILED DESCRIPTION - Production of porous material involves heating citric acid at 200 degrees C, adding sodium hydroxide solution, stirring, dialyzing solution in dialysis bag, filtering, dialyzing filtrate, freeze-drying to obtain brown-yellow graphene quantum dot (GQD) powder, dissolving powder in dimethylformamide solution, adding solution of thionyl chloride, stirring to obtain chlorinated GQD, centrifuging, washing with anhydrous tetrahydrofuran, freeze-drying, heating, centrifuging, washing with absolute ethanol, lyophilizing to obtain GQD-functionalized monomer, adding deionized water, polyvinyl alcohol and hydroquinone, mixing to obtain dispersed phase, stirring, heating, filtering, polymerizing, washing with deionized water and ethanol and drying under vacuum conditions.