• 专利标题:   Synthesis of nano silicon carbide at low temperature used in electric field emission application, involves heat treating clean rice hull in air atmosphere, mixing obtained heat-treated product with mixed salt, magnesium powder, and heat treating in inert atmosphere.
  • 专利号:   CN114735704-A
  • 发明人:   MAO A, FANG D, LIU W, YANG M, YANG X, ZHENG C
  • 专利权人:   UNIV ANHUI TECHNOLOGY
  • 国际专利分类:   B82Y040/00, C01B032/977, C01B032/984, C01B033/021
  • 专利详细信息:   CN114735704-A 12 Jul 2022 C01B-032/977 202285 Chinese
  • 申请详细信息:   CN114735704-A CN10579171 25 May 2022
  • 优先权号:   CN10579171

▎ 摘  要

NOVELTY - Synthesis of nano silicon carbide at low temperature involves carrying out constant-temperature heat treatment of clean rice hulls in air atmosphere to obtain heat treated product containing trace carbon, mixing the product with mixed salt and magnesium powder, carrying out constant-temperature heat treatment in inert atmosphere to obtain heat treated product (A), stirring heat treated product (A) in hydrochloric acid for 3-6 hours, separating, washing and vacuum drying to obtain nano silicon powder containing trace oxygen and carbon, mixing nano silicon powder with carbon source, ball milling for a period of time to obtain silicon and carbon composite material, mixing silicon and carbon composite material with magnesium powder, carrying out constant-temperature heat treatment in inert atmosphere to obtain heat treated product (B), stirring the product (B) in hydrochloric acid for 2-8 hours, separating, washing, and vacuum drying. USE - Synthesis of nano silicon carbide at low temperature uses in electric field emission application, electronic device, microwave absorber, catalyst, capacitor, sensor and biological probe. ADVANTAGE - The method is simple, has high efficiency and less expensive, synthesizes nano silicon carbide at low temperature, using superfine nano-silicon particle powder and graphene oxide prepared by using biomass material as raw material, which can increase the reaction area to reduce the reaction of silicon-carbide synthesis reaction. The method uses rice hull as main raw material, thus contributing the recycling of agricultural waste.