• 专利标题:   Preparing nitrogen-phosphorus co-doped graphene quantum dots by adding 1,3,6-trinitropyrene and co-doping source of nitrogen and phosphorus to water, ultrasonically dispersing mixture, reacting, filtering, dialyzing and freeze-drying.
  • 专利号:   CN110817850-A
  • 发明人:   LI M, GUO Z, WU H, TANG T
  • 专利权人:   UNIV GUILIN TECHNOLOGY
  • 国际专利分类:   B01J027/24, B82Y020/00, C01B032/184, C01B032/194, C09K011/65
  • 专利详细信息:   CN110817850-A 21 Feb 2020 C01B-032/184 202022 Pages: 12 Chinese
  • 申请详细信息:   CN110817850-A CN11331742 21 Dec 2019
  • 优先权号:   CN11331742

▎ 摘  要

NOVELTY - Method for preparing nitrogen-phosphorus co-doped graphene quantum dots involves adding a co-doping source of 1,3,6-trinitropyrene and nitrogen and phosphorus to deionized water at a weight ratio of 1:(20-30), adjusting to a pH of 11-12, ultrasonically dispersing the solution, hydrothermally reacting at 160-200 degrees C for 5-8 hours, cooling, filtering, dialyzing and freeze-drying to obtain the product. USE - The method is useful for preparing nitrogen-phosphorus co-doped graphene quantum dots (claimed). ADVANTAGE - The method avoids introducing impurity atoms, adopts one-step hydrothermal process, is simple in operation and suitable for industrial production, adopts low-cost raw materials and equipment, and provides product having excellent photocatalytic performance.