• 专利标题:   Method for preparing graphene-tin sulfide composite counter electrode material for dye-sensitized photovoltaic cell, involves adding graphene oxide into water, dispersing, adding thiosulfamide followed by cooling, washing and drying.
  • 专利号:   CN105869893-A, CN105869893-B
  • 发明人:   GAO Z, JIANG K, WU D, XU F, WANG L, CHANG J
  • 专利权人:   UNIV HENAN NORMAL, UNIV HENAN NORMAL
  • 国际专利分类:   H01G009/042, H01G009/20
  • 专利详细信息:   CN105869893-A 17 Aug 2016 H01G-009/20 201664 Pages: 11 Chinese
  • 申请详细信息:   CN105869893-A CN10219917 11 Apr 2016
  • 优先权号:   CN10219917

▎ 摘  要

NOVELTY - A graphene-tin sulfide composite counter electrode material preparing method involves adding graphene oxide into deionized water and ultrasonically dispersing homogeneously, and mixing tin tetrachloride pentahydrate and thiourea. Thiosulfamide is added to the solution and stirred to form a homogeneous solution. The resulting homogeneous solution is transferred to a hydrothermal reaction kettle at 120-180 degrees C for 1 to 24 hours, followed by autothermal cooling, washing by water and ethanol, and drying under vacuum oven at 60 degrees C for 24 hours to obtain product. USE - Method for preparing graphene-tin sulfide composite counter electrode material that is utilized in dye-sensitized photovoltaic cell. ADVANTAGE - The material has high charge transfer ability and good catalytic activity, and can be prepared in simple, easy and cost effective manner.