• 专利标题:   Preparation of reinforced polyimide composite material involves dispersing graphene oxide and carboxylated carbon nanotube in organic solution, adding N,N'-dicyclohexylcarbodiimide, dianhydride monomer and diamine monomer and molding.
  • 专利号:   CN108276576-A
  • 发明人:   SHI H, ZHANG Y, WANG H, YU W, LIU B
  • 专利权人:   UNIV TIANJIN POLYTECHNIC
  • 国际专利分类:   C08G073/10, C08J005/18, C08K003/04, C08K007/24, C08K009/02, C08K009/04
  • 专利详细信息:   CN108276576-A 13 Jul 2018 C08G-073/10 201858 Pages: 13 Chinese
  • 申请详细信息:   CN108276576-A CN10105405 02 Feb 2018
  • 优先权号:   CN10105405

▎ 摘  要

NOVELTY - The preparation method of reinforced polyimide composite material involves ultrasonically dispersing graphene oxide and carboxylated carbon nanotube in organic solution, adding N,N'-dicyclohexylcarbodiimide or 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride/N-hydroxysuccinimide condensing agent to the mixture and then stirring, adding organic substance-containing amino groups to the mixture and then reacting at 50-150 degrees C for 1-24 hours, adding dianhydride monomer, diamine monomer and organic solvent to the mixture and then polymerizing, molding the mixture and heat treating. USE - The method is useful for preparation of reinforced polyimide composite material. ADVANTAGE - The method enables preparation of reinforced polyimide composite material with excellent synergistic effect, mechanical properties and thermal stability.